Characterization of Porous Solids VI, Proceedings of the 6 International Symposium on the Characterization of Porous Solids (COPS-VI) 0444512616, 9780444512611, 9780080528915

Table of contents :
Content:
Preface
Page xv
Francisco Rodriguez-Reinoso

Committees
Page xvii

Financial Support
Page xvii

Scanning probe microscopies for the characterization of porous solids: strengths and limitations Original Research Article
Pages 1-10
J.I. Paredes, A. Martínez-Alonso, J.M.D. Tascón

Role of gas adsorption in nanopore characterization Original Research Article
Pages 11-18
K. Kaneko, T. Ohba, Y Hattori, M. Sunaga, H. Tanaka, H. Kanoh

Reconstruction method for the characterization of porous carbons Original Research Article
Pages 19-26
J. Pikunic, C. Clinard, N. Cohaut, K.E. Gubbins, J.-M. Guet, R.J.-M. Pellenq, I. Rannou, J.-N. Rouzaud

A new method for microporosity detection based on the use of the Corrugated Pore Structure Model (CPSM) Original Research Article
Pages 27-34
C.E. Salmas, V.N. Stathopoulos, A.K. Ladavos, P.J. Pomonis, G.P. Androutsopoulos

Physisorption in nanopores of various sizes and shapes : A Grand Canonical Monte Carlo simulation study Original Research Article
Pages 35-42
B. Coasne, A. Grosman, C. Ortega, R.J.M. Pellenq

Induced porosity in cross-linked polymer networks: Mean field theory and simulations Original Research Article
Pages 43-50
Simcha Srebnik

Microbeam small angle X-ray scattering (μSAXS): a novel technique for the characterization of activated carbon fibers Original Research Article
Pages 51-58
D. Lozano-Castelló, E. Raymundo-Piñero, D. Cazorla-Amorós, A. Linares-Solano, M. Müller, C. Riekel

Real time determination of porosity development in carbons: A combined SAXS/TGA approach Original Research Article
Pages 59-66
J.M. Calo, P.J. Hall, S. Houtmann, D.Lozano Castello, R.E. Winans, S. Seifert

SANS investigations of adsorption mechanisms in model porous silicas Original Research Article
Pages 67-74
S. Kallus, A. Hahn, J.D.F. Ramsav

Preparation and surface characterisation of novel ceria-copper and ceria-manganese mixed oxides Original Research Article
Pages 75-82
Maria Christophidou, Chans R. Theocharis

About the exclusive mesoporous character of MCM-41 Original Research Article
Pages 83-90
Á. Berenguer-Murcia, J. García-Martínez, D. Cazorla-Amorós, A. Martínez-Alonso, J.M.D. Tascón, Á. Linares-Solano

Incorporation of appropriate contact angles in textural characterization by mercury porosimetry Original Research Article
Pages 91-98
J.C. Groena, L.A.A. Peffer, J. Pérez-Ramírez

A two-stage Horvath-Kawazoe adsorption model for pore size distribution analysis Original Research Article
Pages 99-106
Robert J. Dombrowski, Christian M. Lastoskie

Textural and chemical characterization of NaX zeolite exchanged with Zn(II) ions Original Research Article
Pages 107-114
J. Silvestre-Albero, A. Sepúlveda-Escribano, F. Rodríguez-Reinoso

Evaluation and comparison of the pore structure and related properties of particulate and monolithic silicas for liquid phase separation processes Original Research Article
Pages 115-122
K.K. Unger, B. Bidlingmaier, C. du Fresne von Hohenesche, D. Lubda

Percolation phenomena in micropore adsorption: Influence on single and multicomponent adsorption equilibria Original Research Article
Pages 123-130
S. Ismadji, S.K. Bhatia

Characterisation of the surface chemistry of activated carbon by molecular simulation of water adsorption Original Research Article
Pages 131-138
M. Jorge, N.A. Seaton

Comparison of porous carbons developed via templating approaches Original Research Article
Pages 139-146
P.M. Barata-Rodrigues, T.J. Mays, N.A. Seaton, G.D. Moggridge

Simulation of adsorption in 3-D reconstructed mesoporous materials by a simulated annealing algorithm Original Research Article
Pages 147-154
M.E. Kainourgiakis, E.S. Kikkinides, G.Ch. Charalambopoulou, A.K. Stubos

Understanding adsorption hysteresis in porous glasses and other mesoporous materials Original Research Article
Pages 155-162
H.-J. Woo, L. Sarkisov, P.A. Monson

Structural studies of mesoporous alumina membranes by small angle X-ray scattering Original Research Article
Pages 163-170
John C. Dore, Robert E. Benfïeld, Didier Grandjean, Günter Schmid, Michael Kröll, David Le Bolloc’h

Assessing microporosity by immersion microcalorimetry into liquid nitrogen or liquid argon Original Research Article
Pages 171-176
Jean Rouquerol, Philip Llewellyn, Ricardo Navarrete, Françoise Rouquerol, Renaud Denoyel

The lower closure point of the adsorption hysteresis loop of fluids in mesoporous silica materials Original Research Article
Pages 177-184
A. Schreiber, S. Reinhardt, G.H. Findenegg

New methodologies in mercury porosimetry Original Research Article
Pages 185-192
Sean P. Rigby

Theoretical calculation of high micropore volumes on activated carbons Original Research Article
Pages 193-200
J. Alcañiz-Monge

Assessment of ultramicroporosity on carbon molecular sieves by water adsorption Original Research Article
Pages 201-208
J. Alcañiz-Monge, D. Lozano-Castelló

Active surface area of carbon materials determined by different methods Original Research Article
Pages 209-216
A. Arenillas, F. Rubiera, J.B. Parra, J.J. Pis

Heterogeneity of sewage sludge derived materials as a factor governing their performance as adsorbents of acidic gases Original Research Article
Pages 217-224
A. Bagreev, S. Bashkova, B. Reznik, V. Zibat, T.J. Bandosz

Evaluation of microporous structure of carbon molecular sieves using the pycnometric method Original Research Article
Pages 225-230
M. Balys, B. Buczek, E. Vogt

Characterization of porous carbonaceous sorbents using adsorption data in wide temperature and pressure ranges Original Research Article
Pages 231-238
Guy De Weireld, Marc Frère

Ammonia accessibility to the porosity of several activated carbons measured by flow adsorption microcalorimetry Original Research Article
Pages 239-246
M. Domingo-García, A.J. Groszek, F.J. López-Garzón, M. Pérez-Mendoza

An IGC and TA study of acetaldehyde adsorption on activated carbons Original Research Article
Pages 247-254
Y. El-Sayed, T.J. Bandosz

A novel approach for characterising carbon catalysts by TAP experiments Original Research Article
Pages 255-260
V. Fierro, M.T. Izquierdo, Y. Schuurmar, B. Rubio, C. Mirodatos

Preparation of activated carbons with controlled pore size Original Research Article
Pages 261-265
M.M.A. Freitas, J.L. Figueiredo

Characterization of porous solids using low pressure VOC adsorption data Original Research Article
Pages 267-274
Joëlle Nokennan, Sébastien Dutour, Marc Frère, Sophie Limborg-Noetinger, Sophie Jullian

Energetics and mechanism of physical sorption by carbonaceous solids: Evaluation of surface area and porosity factors Original Research Article
Pages 275-282
E. Loren Fuller Jr.

Phenanthrene asorption on a carbonaceous material: Moisture and CO2 influence Original Research Article
Pages 283-290
A.M. Mastral, T García, R Murillo, M.S. Callén, J.M. López, M.V. Navarro

Water adsorption on micro and mesoporous silicas Original Research Article
Pages 291-298
J. Alcañiz-Monge, D. Lozano-Castelló

The effect of surface functionalization of mesoporous silicas with propylimidazol on porosity, pore connectivity and tortuosity Original Research Article
Pages 299-306
G.S. Armatas, C.E. Salmas, G.P. Androutsopoulos, P.J. Pomonis

Preparation of porous silica by acid activation of metakaolins Original Research Article
Pages 307-314
C. Belver, M.A. Bañares, M.A. Vicente

The effect of particle shape on the filtration rate and shear strength of quartz and dolomite mineral filter cakes Original Research Article
Pages 315-322
B. Benli Gönül, Ö. Özcan

Characterisation of silica low-density xerogels in presence of additives by image analysis and nitrogen adsorption-desorption Original Research Article
Pages 323-330
S. Blacher, C. Alié, C. Gommes, P. Lodewyckx, R. Pirard, J.-P. Pirard

Texture characterization of ultramacroporous materials using non-destructive methods Original Research Article
Pages 331-338
S. Blacher, V. Maquet, A. Léonard, G. Chapelle, M. Crine, R. Jérôme, J.-P. Pirard

Formation of hierarchically ordered silicas prepared by spray drying of nanosized spheres Original Research Article
Pages 339-346
C. du Fresne von Hohenesche, V. Stathopoulos, K.K. Unger, A. Lind, M. Lindén

Ultrathin porous glass membranes with controlled texture properties Original Research Article
Pages 347-354
D. Enke, F. Friedel, F. Janowski, T. Hahn, W. Gille, R. Müller, H. Kaden

Reconstruction of the mesoporous silica glass Gelsil®50 Original Research Article
Pages 355-362
N. Eschricht, E. Hoinkis, F. Mädler, P. Schubert-Bischoff

Pore structural characteristics of mesostructured materials prepared under different conditions Original Research Article
Pages 363-370
A. Estêvão Candeias, M.M.L. Ribeiro Carrott, P.J.M. Carrott, K. Schumacher, M. Griin, K.K. Unger

A grand canonical Monte Carlo simulation study of water adsorption in a Vycor-like disordered mesoporous material at 300 K Original Research Article
Pages 371-378
J. Puibasset, R.J.-M. Pellenq

A review of the application of the BET equation to experimental data: the C parameter Original Research Article
Pages 379-386
F. Salvador, C. Sánchez-Jiménez, M.J. Sánchez-Montero, A. Salvador

Thermogravimetric and sorption measurement techniques/instruments Original Research Article
Pages 387-394
Jürgen U. Keller, Erich Robens, Cedric du Fresne von Hohenesche

Influence of method of washcoat preparation on hydrothermal stability of alumina support Original Research Article
Pages 395-401
M. Kulazyński, J. Trawczyński, J. Walendziewski

Limestone influence on PAH emissions from coal AFBC. Catalytic or/and adsorption effect? Original Research Article
Pages 403-409
A.M. Mastral, T García, M.S. Callén, J.M. López, R Murillo, M.V. Navarro

Freezing point elevation in nanospace detected directly by atomic force microscopy Original Research Article
Pages 411-418
M. Miyahara, M. Sakamoto, H. Kanda, K. Higashitani

Is it possible to obtain a coherent image of the texture of a porous material? Original Research Article
Pages 419-426
Francis Noville, Cédric Gommes, Catherine Doneux, Alain Brasseur, Renë Pirard, Jean-Paul Pirard

Preparation and characterisation of Cr-Co spinels for methane oxidation in presence of sulphur compounds Original Research Article
Pages 427-434
J.R. Paredes, S. Ordóñez, F.V. Díez, H Sastre

Characterising the porous structure of Egyptian mortars using thermoporometry, mercury intrusion porometry and gas adsorption manometry Original Research Article
Pages 435-441
Jehane Ragaï, Thomas Poyet, Isabelle Beurroies, Françoise Rouquerol, Philip Llewellyn

Monitoring fast pressure changes in gas transport and sorption analysis Original Research Article
Pages 443-449
G. Reichenauer, H.-J. Fella, J. Fricke

Effect of coke deposition on catalyst texture during catalytic cracking reaction Original Research Article
Pages 451-458
J.P. Reymond, C. Delattre, M. Forissier

Precision of porosity measurements on cementitious mortars Original Research Article
Pages 459-466
K. Rübner, Th. Fritz, F. Jacobs

Freezing in mesopores: Aniline in silica glasses and MCM-41 Original Research Article
Pages 467-474
M. Sliwinska-Bartkowiak, G. Dudziak, R. Radhakrishnan, K.E. Gubbins

Transport characteristics of porous solids derived from Chromatographie measurements Original Research Article
Pages 475-482
O. àolcová, P. Schneider

Effects of porous solid structures on the electrical behaviour : Prediction key of transport properties in sedimentary reservoir rock Original Research Article
Pages 483-490
A. Cerepi, R. Burlot, S. Galaup, J-P. Barde, C. Loisy, L. Humbert

Pore and surface characteristics of porous melamine- and phenolic-formaldehyde polymers by sorption and XPS measurements Original Research Article
Pages 491-498
A. Derylo-Marczewska, J. Goworek

Porous structure of multifunctional mineral — carbon and zeolite-carbon sorbents Original Research Article
Pages 499-506
E.B. Drąg, M. Kułazyński, J. Kaczmarczyk

Waste air cleaning using activated carbon fibre cloths regenerable by direct electric heating Original Research Article
Pages 507-513
E. Schippert, C. Möhner, B. Pannwitt, Horst Chmiel

Adsorption of inflammatory cytokines and endotoxin by mesoporous polymers and activated carbons Original Research Article
Pages 515-520
M.C. Murphy, S. Patel, G.J. Phillips, J.G. Davies, A.W. Lloyd, V.M. Gun'ko, S.V. Mikhalovsky

Separation of adsorption isotherms of N2 in internal and interstitial nanopores of single-walled carbon nanohorn — A comparative study with experiment and simulation Original Research Article
Pages 521-527
T. Ohba, H. Kanoh, K. Murata, M. Yudasaka, S. Iijima, K. Kaneko

Visualizing the porous structure of different carbon materials: a scanning tunneling microscopy study Original Research Article
Pages 529-536
J.I. Paredes, A. Martinez-Alonso, J.M.D. Tascón

Textural characterisation of activated carbons obtained from poly(ethylene terephthalate) by carbon dioxide activation Original Research Article
Pages 537-543
J.B. Parra, C.O. Ania, A. Arenillas, J.J. Pis

A Monte Carlo study on the structure of carbon dioxide adsorbed in microporous carbons Original Research Article
Pages 545-552
Th.A. Steriotis, G.K. Papadopoulos, A.K. Stubos, N. Kanellopoulos

Preloading of GAC by natural organic matter: effect of surface chemistry on TCE uptake Original Research Article
Pages 553-560
James E. Kilduff, Reena Srivastava, Tanju Karanfil

Structural studies of saccharose- and anthracene-based carbons by high energy X-ray scattering Original Research Article
Pages 561-568
A. Szczygielska, A. Burian, S. Duber, J.C. Dore, V. Honkimaki

The dynamic adsorption behaviour of volatile organic compounds on activated carbon honeycomb monoliths Original Research Article
Pages 569-576
M. Yates, J. Blanco, M.A. Martín-Luengo

Structural properties of Cu-MCM-41 and Cu-Al-MCM-41(Si/Al=30) catalysts Original Research Article
Pages 577-584
Giovanni Ferraris, Giuliano Moretti, Giuseppe Fierro, Mariano Lo Jacono

Comparative study of the textural properties of alumina-pillared saponites synthesised from the intercalation with various aluminium oligomers Original Research Article
Pages 585-592
L.M. Gandia, M.A. Vicente, A. Gil

Chord length distribution and pore size distribution of porous VYCOR glass Original Research Article
Pages 593-600
W. Gille, D. Enke, F. Janowski

A structural study of dehydration/rehydration of tobermorite, a model cement compound Original Research Article
Pages 601-608
A. Gmira, R.J.-M. Pellenq, I. Rannou, L. Duclaux, C. Clinard, T. Cacciaguerra, N. Lequeux, H. Van Damme

Support mesoporosity: a tool for better control of catalytic behavior of cobalt supported Fischer Tropsch catalysts Original Research Article
Pages 609-616
A. Griboval-Constant, A.Y. Khodakov, R. Bechara, V.L. Zholobenko

Textural characterization of montmorillonite pillared with aluminum/lanthanum polyoxycations Original Research Article
Pages 617-624
J.A. Morante, C. Pesquera, C. Blanco, F. González

Influence of pH in mesoporous silica aluminas (MSA) synthesis Original Research Article
Pages 625-632
C. Rizzo, A. Carati, C. Barabino, C. Perego, G. Bellussi

The adsorption of 1-hexene and 3,3-dimethyl-1-butene on Ru-MCM 41 Original Research Article
Pages 633-638
Udayshanker Singh, Ruth T. Williams, Ian D. Salter

XPS studies of MCM 41 postmodified by a Schiff base copper complex Original Research Article
Pages 639-646
Udayshanker Singh, Ruth T. Williams, Ian D. Salter, Keith R. Hallam, Geoffrey C. Allen

Influence of synthesis conditions on surface heterogeneity of M41 type materials studied with lattice Monte Carlo Original Research Article
Pages 647-654
Flor R. Siperstein, Keith E. Gubbins

Porosity of chemically modified silica gels by nitrogen adsorption, positron annihilation and small angle X-ray scattering Original Research Article
Pages 655-662
J. Goworek, A. Borówka, S. Pikus, J. Wawryszczuk

Preparation and characterization of porous sorbents for hot gas desulfurization Original Research Article
Pages 663-670
F. Tomás Alonso, I. Orenes Fernández, J.M. Palacios Latasa

Synthesis and characterization of MWW zeolites Original Research Article
Pages 671-675
L.M. Vtjurina, S.S. Khvoshchev

Structural analysis of oxyanion — Cation complexes anchored by organic group in mesoporous silicas Original Research Article
Pages 677-684
Hideaki Yoshitake, Toshiyuki Yokoi, Takashi Tatsumi

Adsorption equilibrium of polar/non-polar mixtures on MCM-41: experiments and Monte Carlo simulation Original Research Article
Pages 685-692
J.-H. Yun., Y. He, M. Otero, T. Düren, N.A. Seaton

Nondestructive characterization of porous ceramics by X-Ray refraction Original Research Article
Pages 693-699
K.-W. Harbich, F.E. Fensch-Kleemann, B. Röhl-Kuhn, P. Klobes

Ion-exchange properties of a novel layered titanium(IV) phosphate Original Research Article
Pages 701-708
O.A. Khainakova, A. Espina, C. Trobajo, S.A. Khainakov, J.R. García, A.I. Bortun

The Anomalous sorptive behaviour of Zsm-5 and silicalite-I: Observation of low-pressure hysteresis in nitrogen adsorption Original Research Article
Pages 709-716
Georgia Kyriakou, Chans R. Theocharis

Characterisation of the textural properties of chemically dealuminated Y zeolites Original Research Article
Pages 717-722
R. López-Fonseca, B. de Rivas, J.I. Gutiérrez-Ortiz, J.R. González-Velasco

Complementarity of microcalorimetry, manometry and gravimetry in the study of gas adsorption by microporous solids up to 50 bar Original Research Article
Pages 723-729
Stéphanie Moret, Thomas Poyet, David Bigot, Bernd Polster, Simon Crispel, Jean Rouquerol, Philip Llewellyn

The applicability of the Dubinin-Radushkevich equation to the very low pressure region of isotherms of various microporous solids Original Research Article
Pages 731-735
P. Lodewyckx, L. Verhoeven

Controlled porosity and surface area titania gels as novel photocatalytic washcoats Original Research Article
Pages 737-744
M. Yates, E. Garcia

The effect of geometry and axial orientation of spheroidal particles on the adsorption rate in a granular porous medium Original Research Article
Pages 745-751
F.A. Coutelieris

The effect of Peclet on the Sherwood number in high porosity granular media Original Research Article
Pages 753-760
F.A. Coutelieris, M.E. Kainourgiakis, A.K. Stubos