Carbohydrate Analysis by Modern Chromatography and Electrophoresis 0444500618, 9780444500618

Table of contents :
Content:
Preface
Pages V-VII
Ziad El Rassi

List of contributors
Pages IX-XIII

Chapter 1 Preparation of carbohydrates for analysis by modern chromatography and electrophoresis Original Research Article
Pages 3-38
A.J. Mort, M.L. Pierce

Chapter 2 Reversed-phase and hydrophobic interaction chromatography of carbohydrates and glycoconjugates Original Research Article
Pages 41-102
Ziad El Rassi

Chapter 3 HPLC of carbohydrates on graphitized carbon columns Original Research Article
Pages 103-119
Kyoko Koizumi

Chapter 4 High performance hydrophilic interaction chromatography of carbohydrates with polar sorbents Original Research Article
Pages 121-163
Shirley C. Churms

Chapter 5 HPLC of carbohydrates with cation- and anion-exchange silica and resin-based stationary phases Original Research Article
Pages 165-205
Christian W. Huck, Christian G. Huber, Günther K. Bonn

Chapter 6 High-performance anion-exchange chromatography of carbohydrates on pellicular resin columns Original Research Article
Pages 207-250
Ye Zhang, Y.C. Lee

Chapter 7 Lectin-affinity chromatography of carbohydrates Original Research Article
Pages 251-265
Tamao Endo

Chapter 8 Modern size-exclusion chromatography of carbohydrates and glycoconjugates Original Research Article
Pages 267-303
Shirley C. Churms

Chapter 9 Molar mass determination of complex bioglycopolymers by size exclusion chromatography and light scattering detection Original Research Article
Pages 305-345
K. Jumel

Chapter 10 Multi-dimensional mapping of N-linked glycans by HPLC Original Research Article
Pages 347-385
Noriko Takahashi

Chapter 11HPLC analysis of oligosaccharides derived from glycosaminoglycans in biological materials Original Research Article
Pages 387-402
Toshio Imanari, Toshihiko Toida, Ichiro Koshiishi, Hidenao Toyoda

Chapter 12 Starch chain length analysis by using an anion-exchange chromatography system equipped with an enzyme reactor and a PAD detector Original Research Article
Pages 403-422
Kit-Sum Wong, Jay-Lin Jane

Chapter 13 TLC and HPLC of glycosphingolipids Original Research Article
Pages 423-482
Johannes Müthing

Chapter 14 Analysis of carbohydrates in food and beverages by HPLC and CE Original Research Article
Pages 483-502
Tomoyoshi Soga

Chapter 15 Preparative HPLC of carbohydrates Original Research Article
Pages 505-534
Kevin B. Hicks, Arland T. Hotchkiss Jr.

Chapter 16 Preparative purification and utilization of tyrosinamide N-Glycan libraries Original Research Article
Pages 535-570
Kevin G. Rice, V. Hayden Thomas, Wendy T. Collard

Chapter 17 Field-flow fractionation for molar mass characterization of polysaccharides Original Research Article
Pages 573-594
Karl-Gustav Wahlund

Chapter 18 Capillary electrophoresis and electrochromatography of carbohydrates Original Research Article
Pages 597-676
Ziad El Rassi

Chapter 19 Studies on carbohydrate-Protein interaction by high performance capillary affinity electrophoresis Original Research Article
Pages 677-690
Susumu Honda, Atsushi Taga

Chapter 20 Analysis of glycoproteins and their glycopeptide and glycan fragments by electrophoresis and capillary electrophoresis Original Research Article
Pages 691-785
Nguyet Thuy Tran, Marion Cabanes-Macheteau, Myriam Taverna

Chapter 21 Fluorphore-assisted carbohydrate electrophoresis (FACE®): Rapid enzymatic analysis of oligosaccharide mixtures from recombinant glycoproteins for batch comparability Original Research Article
Pages 787-798
C. Hague, I. Masada, B.K. Brandley

Chapter 22 Capillary electrophoresis of intact and depolymerized glycosaminoglycans and proteoglycans Original Research Article
Pages 799-826
Nikos K. Karamanos, Anders Hjerpe

Chapter 23 A current perspective on analysis of sugar monomers using GC-MS and GC-MS/MS Original Research Article
Pages 829-843
Alvin Fox

Chapter 24 Gas chromatography-mass spectrometric analysis of monosaccharides after methanolysis and trimethylsilylation. Potential for the characterization of substances of vegetal origin: Application to the study of museum objects Original Research Article
Pages 845-902
P. Mejanelle, J. Bleton, A. Tchapla, S. Goursaud

Chapter 25 Pulsed electrochemical detection of carbohydrates at noble metal electrodes following liquid chromatographic and electrophoretic separation Original Research Article
Pages 905-946
William R. Lacourse

Chapter 26 Electrochemical detection of carbohydrates at constant potential after HPLC and CE separations Original Research Article
Pages 947-959
Richard P. Baldwin

Chapter 27 Mass spectrometry of oligosaccharides Original Research Article
Pages 961-1042
Mark Stahl, Alexander Von Brocke, Ernst Bayer

Chapter 28 Pre- and post-column detection-oriented derivatization techniques in HPLC of carbohydrates Original Research Article
Pages 1043-1069
Sumihiro Hase

Chapter 29 Enzyme reactors and enzyme electrodes for the liquid chromatographic determination of carbohydrates Original Research Article
Pages 1071-1100
L.J. Nagels

Chapter 30 Carbohydrate analysis by LC and SFC using evaporative light scattering detection Original Research Article
Pages 1101-1134
M. Lafosse, B. Herbreteau

Chapter 31 Chiroptical detectors for HPLC of carbohydrates Original Research Article
Pages 1135-1149
Neil Purdie

Author index
Pages 1151-1196

Subject index
Pages 1197-1223